Crystal structure of 1-[4-(2,2-diphenylacetyl)piperazin-1-yl]-3-buten-2-ol

Yoshiyuki Miyata; Yumiko Osa; Yoko Sato; Kouichi Takino; Seiki Kobayashi; Tutomu Takeuchi; Hiroaki Takayanagi

doi:10.2116/analscix.20.x33

Crystal structure of 1-[4-(2,2-diphenylacetyl)piperazin-1-yl]-3-buten-2-ol

Yoshiyuki Miyata
, Yumiko Osa
, Yoko Sato
, Kouichi Takino
, Seiki Kobayashi
, Tutomu Takeuchi
, Hiroaki Takayanagi

Department of Infectious Diseases

Research output: Contribution to journal › Comment/debate › peer-review

Abstract

1-[4-(2,2-Diphenylacetyl)piperazin-1-yl]-3-buten-2-ol (1) crystallizes in the monoclinic space group P2₁/a with a = 18.057(1), b = 6.036(2), c = 19.309(1)Å, β = 115.630(4)°, V = 1897.3(5)Å³, Z = 4. The carbonyl group and the nitrogen of piperazine constitutes an almost planar amide moiety due to being conjugated with the carbonyl group. An intermolecular hydrogen interaction of the hydroxyl group to another nitrogen of piperazine (bond distance: 2.86(3)Å) is present. 2004

Original language	English
Pages (from-to)	x33-x34
Journal	Analytical Sciences: X-ray Structure Analysis Online
Volume	20
Issue number	2
DOIs	https://doi.org/10.2116/analscix.20.x33
Publication status	Published - 2004

ASJC Scopus subject areas

Analytical Chemistry
Materials Chemistry

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10.2116/analscix.20.x33

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@article{d0413eba74464f358fb1542a08cfd5cc,

title = "Crystal structure of 1-[4-(2,2-diphenylacetyl)piperazin-1-yl]-3-buten-2-ol",

abstract = "1-[4-(2,2-Diphenylacetyl)piperazin-1-yl]-3-buten-2-ol (1) crystallizes in the monoclinic space group P21/a with a = 18.057(1), b = 6.036(2), c = 19.309(1){\AA}, β = 115.630(4)°, V = 1897.3(5){\AA}3, Z = 4. The carbonyl group and the nitrogen of piperazine constitutes an almost planar amide moiety due to being conjugated with the carbonyl group. An intermolecular hydrogen interaction of the hydroxyl group to another nitrogen of piperazine (bond distance: 2.86(3){\AA}) is present. 2004",

author = "Yoshiyuki Miyata and Yumiko Osa and Yoko Sato and Kouichi Takino and Seiki Kobayashi and Tutomu Takeuchi and Hiroaki Takayanagi",

year = "2004",

doi = "10.2116/analscix.20.x33",

language = "English",

volume = "20",

pages = "x33--x34",

journal = "Analytical Sciences: X-ray Structure Analysis Online",

issn = "1348-2238",

publisher = "Japan Society for Analytical Chemistry",

number = "2",

}

TY - JOUR

T1 - Crystal structure of 1-[4-(2,2-diphenylacetyl)piperazin-1-yl]-3-buten-2-ol

AU - Miyata, Yoshiyuki

AU - Osa, Yumiko

AU - Sato, Yoko

AU - Takino, Kouichi

AU - Kobayashi, Seiki

AU - Takeuchi, Tutomu

AU - Takayanagi, Hiroaki

PY - 2004

Y1 - 2004

N2 - 1-[4-(2,2-Diphenylacetyl)piperazin-1-yl]-3-buten-2-ol (1) crystallizes in the monoclinic space group P21/a with a = 18.057(1), b = 6.036(2), c = 19.309(1)Å, β = 115.630(4)°, V = 1897.3(5)Å3, Z = 4. The carbonyl group and the nitrogen of piperazine constitutes an almost planar amide moiety due to being conjugated with the carbonyl group. An intermolecular hydrogen interaction of the hydroxyl group to another nitrogen of piperazine (bond distance: 2.86(3)Å) is present. 2004

AB - 1-[4-(2,2-Diphenylacetyl)piperazin-1-yl]-3-buten-2-ol (1) crystallizes in the monoclinic space group P21/a with a = 18.057(1), b = 6.036(2), c = 19.309(1)Å, β = 115.630(4)°, V = 1897.3(5)Å3, Z = 4. The carbonyl group and the nitrogen of piperazine constitutes an almost planar amide moiety due to being conjugated with the carbonyl group. An intermolecular hydrogen interaction of the hydroxyl group to another nitrogen of piperazine (bond distance: 2.86(3)Å) is present. 2004

UR - https://www.scopus.com/pages/publications/70450279107

UR - https://www.scopus.com/pages/publications/70450279107#tab=citedBy

U2 - 10.2116/analscix.20.x33

DO - 10.2116/analscix.20.x33

M3 - Comment/debate

AN - SCOPUS:70450279107

SN - 1348-2238

VL - 20

SP - x33-x34

JO - Analytical Sciences: X-ray Structure Analysis Online

JF - Analytical Sciences: X-ray Structure Analysis Online

IS - 2

ER -

Crystal structure of 1-[4-(2,2-diphenylacetyl)piperazin-1-yl]-3-buten-2-ol

Abstract

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