Homogenization and particle size reduction of PbTiO3 by ball-milling of precursor gels

Katsuhiko Takeuchi; Tetsuhiko Isobe; Mamoru Senna

doi:10.1006/jssc.1994.1119

Homogenization and particle size reduction of PbTiO₃ by ball-milling of precursor gels

Katsuhiko Takeuchi
, Tetsuhiko Isobe
, Mamoru Senna

Department of Applied Chemistry

Research output: Contribution to journal › Article › peer-review

10 Citations (Scopus)

Abstract

Ball-milling of mixed gel derived from a simple mixing of component alkoxides increased the compositional microhomogeneity, judged quantitatively by high-resolution microprobe chemical analysis. At the same time, the particle size of PbTiO₃ obtained after calcination at 1023 K for 2 hr in air decreased, approaching those of oxide fine particles delivered from a bidentate alkoxide through an identical thermal treatment.

Original language	English
Pages (from-to)	401-405
Number of pages	5
Journal	Journal of Solid State Chemistry
Volume	109
Issue number	2
DOIs	https://doi.org/10.1006/jssc.1994.1119
Publication status	Published - 1994 Apr

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Condensed Matter Physics
Physical and Theoretical Chemistry
Inorganic Chemistry
Materials Chemistry

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10.1006/jssc.1994.1119

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abstract = "Ball-milling of mixed gel derived from a simple mixing of component alkoxides increased the compositional microhomogeneity, judged quantitatively by high-resolution microprobe chemical analysis. At the same time, the particle size of PbTiO3 obtained after calcination at 1023 K for 2 hr in air decreased, approaching those of oxide fine particles delivered from a bidentate alkoxide through an identical thermal treatment.",

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AB - Ball-milling of mixed gel derived from a simple mixing of component alkoxides increased the compositional microhomogeneity, judged quantitatively by high-resolution microprobe chemical analysis. At the same time, the particle size of PbTiO3 obtained after calcination at 1023 K for 2 hr in air decreased, approaching those of oxide fine particles delivered from a bidentate alkoxide through an identical thermal treatment.

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Homogenization and particle size reduction of PbTiO₃ by ball-milling of precursor gels

Abstract

ASJC Scopus subject areas

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