Synthetic studies on altohyrtins (spongistatins): Synthesis of the C1- C14 (AB) spiroacetal portion

Takeshi Terauchi; Masaya Nakata

doi:10.1016/S0040-4039(98)00619-4

Synthetic studies on altohyrtins (spongistatins): Synthesis of the C1- C14 (AB) spiroacetal portion

Takeshi Terauchi, Masaya Nakata

Department of Applied Chemistry

Research output: Contribution to journal › Article › peer-review

33 Citations (Scopus)

Abstract

The C1-C14 portion of altohyrtins (spongistatins) was prepared in a convergent manner from 3,4,6-tri-O-acetyl-D-glucal via a chelation-controlled methylation of ketone, dithiane couplings with epoxides, and a thermodynamically-controlled spitoacetalization.

Original language	English
Pages (from-to)	3795-3798
Number of pages	4
Journal	Tetrahedron Letters
Volume	39
Issue number	22
DOIs	https://doi.org/10.1016/S0040-4039(98)00619-4
Publication status	Published - 1998 May 28

ASJC Scopus subject areas

Biochemistry
Drug Discovery
Organic Chemistry

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10.1016/S0040-4039(98)00619-4

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abstract = "The C1-C14 portion of altohyrtins (spongistatins) was prepared in a convergent manner from 3,4,6-tri-O-acetyl-D-glucal via a chelation-controlled methylation of ketone, dithiane couplings with epoxides, and a thermodynamically-controlled spitoacetalization.",

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AB - The C1-C14 portion of altohyrtins (spongistatins) was prepared in a convergent manner from 3,4,6-tri-O-acetyl-D-glucal via a chelation-controlled methylation of ketone, dithiane couplings with epoxides, and a thermodynamically-controlled spitoacetalization.

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Synthetic studies on altohyrtins (spongistatins): Synthesis of the C1- C14 (AB) spiroacetal portion

Abstract

ASJC Scopus subject areas

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