抄録
A method for simultaneous determination of metribuzin (MET) and three metribuzin metabolites in livestock products and seafoods by liquid chromatography-tandem mass spectrometry (LC-MS/MS) was developed. MET and its metabolites were extracted from a sample with acetonitrile, followed by InertSepC18 and BondElut SAX cartridge cleanup. The LC separation was performed on a C18 column using 0.01 mol/L ammonium formate-acetonitrile-methanol (70 : 21 : 9) as the mobile phase and MS detection with both positive and negative ion electrospray ionization. The mean recoveries from 10 livestock products and seafoods were generally >60%, and the relative standard deviations were <20%.
本文言語 | English |
---|---|
ページ(範囲) | 28-33 |
ページ数 | 6 |
ジャーナル | Journal of the Food Hygienic Society of Japan |
巻 | 52 |
号 | 1 |
DOI | |
出版ステータス | Published - 2011 2月 |
ASJC Scopus subject areas
- 食品科学
- 公衆衛生学、環境および労働衛生