Analysis of metribuzin and its metabolites in livestock products and seafoods by liquid chromatography-tandem mass spectrometry

Shigemi Kai, Takeshi Akaboshi, Masumi Waki, Teruhisa Fuzimaki, Hideko Kanazawa

研究成果: Article査読

3 被引用数 (Scopus)

抄録

A method for simultaneous determination of metribuzin (MET) and three metribuzin metabolites in livestock products and seafoods by liquid chromatography-tandem mass spectrometry (LC-MS/MS) was developed. MET and its metabolites were extracted from a sample with acetonitrile, followed by InertSepC18 and BondElut SAX cartridge cleanup. The LC separation was performed on a C18 column using 0.01 mol/L ammonium formate-acetonitrile-methanol (70 : 21 : 9) as the mobile phase and MS detection with both positive and negative ion electrospray ionization. The mean recoveries from 10 livestock products and seafoods were generally >60%, and the relative standard deviations were <20%.

本文言語English
ページ(範囲)28-33
ページ数6
ジャーナルJournal of the Food Hygienic Society of Japan
52
1
DOI
出版ステータスPublished - 2011 2月

ASJC Scopus subject areas

  • 食品科学
  • 公衆衛生学、環境および労働衛生

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