Novel C-3 Epimerization of Digitoxosides to Olivosides under Hydrogenolysis Conditions

Kazunobu Toshima; Kyoko Inagaki; Masaya Nakata; Shuichi Matsumura

doi:10.1055/s-1997-3269

Novel C-3 Epimerization of Digitoxosides to Olivosides under Hydrogenolysis Conditions

Kazunobu Toshima, Kyoko Inagaki, Masaya Nakata, Shuichi Matsumura

応用化学科

研究成果: Article › 査読

2 被引用数 (Scopus)

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The treatment of several β-digitoxosides with hydrogen in the presence of a catalytic amount of Raney-Ni (W4) in MeOH at 50°C under neutral conditions afforded the C-3 epimers, β-olivosides, in good yields.

本文言語	English
ページ（範囲）	695-696
ページ数	2
ジャーナル	Synlett
巻	1997
号	6
DOI	https://doi.org/10.1055/s-1997-3269
出版ステータス	Published - 1997 1月 1

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有機化学

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10.1055/s-1997-3269

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title = "Novel C-3 Epimerization of Digitoxosides to Olivosides under Hydrogenolysis Conditions",

abstract = "The treatment of several β-digitoxosides with hydrogen in the presence of a catalytic amount of Raney-Ni (W4) in MeOH at 50°C under neutral conditions afforded the C-3 epimers, β-olivosides, in good yields.",

author = "Kazunobu Toshima and Kyoko Inagaki and Masaya Nakata and Shuichi Matsumura",

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AB - The treatment of several β-digitoxosides with hydrogen in the presence of a catalytic amount of Raney-Ni (W4) in MeOH at 50°C under neutral conditions afforded the C-3 epimers, β-olivosides, in good yields.

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Novel C-3 Epimerization of Digitoxosides to Olivosides under Hydrogenolysis Conditions

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