Simple syntheses of 3,4-dideoxy-oct-2-ulosonic acids

Tony K.M. Shing

doi:10.1016/S0040-4039(00)91608-3

Simple syntheses of 3,4-dideoxy-oct-2-ulosonic acids

Tony K.M. Shing

化学科

研究成果: Article › 査読

12 被引用数 (Scopus)

抄録

Bisacetonated aldehydo-d-arabinose has been converted by three consecutive reactions (Wittig reaction, catalytic hydrogenation, and hydrolysis) into 3,4-dideoxy-d-arabino-oct-2-ulosonic acid (4-deoxy-KDO), isolated as its calcium salt in an overall yield of 37% from d-arabinose. Likewise reactions of d-xylose gave calcium 3,4-dideoxy-d-xylo-oct-2-ulosonate in an overall yield of 34%.

本文言語	English
ページ（範囲）	1307-1308
ページ数	2
ジャーナル	Tetrahedron Letters
巻	33
号	10
DOI	https://doi.org/10.1016/S0040-4039(00)91608-3
出版ステータス	Published - 1992 3月 3

ASJC Scopus subject areas

生化学
創薬
有機化学

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10.1016/S0040-4039(00)91608-3

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abstract = "Bisacetonated aldehydo-d-arabinose has been converted by three consecutive reactions (Wittig reaction, catalytic hydrogenation, and hydrolysis) into 3,4-dideoxy-d-arabino-oct-2-ulosonic acid (4-deoxy-KDO), isolated as its calcium salt in an overall yield of 37\% from d-arabinose. Likewise reactions of d-xylose gave calcium 3,4-dideoxy-d-xylo-oct-2-ulosonate in an overall yield of 34\%.",

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N2 - Bisacetonated aldehydo-d-arabinose has been converted by three consecutive reactions (Wittig reaction, catalytic hydrogenation, and hydrolysis) into 3,4-dideoxy-d-arabino-oct-2-ulosonic acid (4-deoxy-KDO), isolated as its calcium salt in an overall yield of 37% from d-arabinose. Likewise reactions of d-xylose gave calcium 3,4-dideoxy-d-xylo-oct-2-ulosonate in an overall yield of 34%.

AB - Bisacetonated aldehydo-d-arabinose has been converted by three consecutive reactions (Wittig reaction, catalytic hydrogenation, and hydrolysis) into 3,4-dideoxy-d-arabino-oct-2-ulosonic acid (4-deoxy-KDO), isolated as its calcium salt in an overall yield of 37% from d-arabinose. Likewise reactions of d-xylose gave calcium 3,4-dideoxy-d-xylo-oct-2-ulosonate in an overall yield of 34%.

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U2 - 10.1016/S0040-4039(00)91608-3

DO - 10.1016/S0040-4039(00)91608-3

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JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 10

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Simple syntheses of 3,4-dideoxy-oct-2-ulosonic acids

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